HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethyl Sulfide → Trimethylsulfonium Triflate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethyl Sulfide | HCID 1068 | — |
| Reactant | Methyl triflate | HCID 9526 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | Trimethylsulfonium Triflate | HCID 10933171 | — |
Reaction Steps
16 mmol of dimethyl sulfide was dissolved in 10 ml of dichloromethane at 0° C., and about 17 mmol of methyltrifluoromethane sulfonate was slowly dripped to the mixture to obtain a white solid product. The solid product was filtered and dried for 1 hour in an oven at 50° C. to obtain the following product:
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08536347B2 |
| Source dataset | uspto-grants-2013_09 |
| ORD ID | ord-5cc9413dfef7447db1b13d03a866a5a8 |
| Source note | uspto-grants-2013_09 |