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HRID 432936作成日:2026年10月26日

4-(3-Bromo-4-methoxyphenoxy)-3,5-dimethylnitrobenzene → 4-(3-Bromo-4-methoxy-phenoxy)-3,5-dimethyl-phenylamine

https://huagongshe.com/reaction/432936

反応式

関与物質

役割名称HCID仕込み量
反応物4-(3-Bromo-4-methoxyphenoxy)-3,5-dimethylnitrobenzeneHCID 22339728—
触媒PalladiumHCID 23938—
溶媒Ethyl AcetateHCID 8857—
生成物4-(3-Bromo-4-methoxy-phenoxy)-3,5-dimethyl-phenylamineHCID 2233950294%

反応手順

A mixture of the title product of Step A (5.0 g) and 10% palladium on carbon (0.6 g) in ethyl acetate (100 ml) was hydrogenated at 50 psi for 3 h. The reaction was filtered through Celite and concentrated to afford the title compound of Step B as a yellow solid (4.3 g). MS (APCl+) Calc: 321; Found 322 (M+1).

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US06664291B2
出典データセットuspto-grants-2003_12
ORD IDord-414a861130a146b7acaea4be7d466a07
出典メモuspto-grants-2003_12