HuagongsheHuagongshe Chemistry Print Report · For research reference only
p-Toluidine → 2-hydroxy-N-(4-methylphenyl)benzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | p-Toluidine | HCID 7813 | — |
| Reactant | Phenyl Salicylate | HCID 8361 | — |
| Product | 2-hydroxy-N-(4-methylphenyl)benzamide | HCID 478805 | — |
Reaction Steps
The 4′-methyl-salicylanilide was prepared by condensing phenyl salicylate with 4-toluidine then purified as described in Example 2a. A ligand mixture was then prepared from 4′-methyl-salicylanilide and binaphthol using the procedure described in Example 5a. 31P NMR (121.77 MHz): several peaks between 117.1-117.8 ppm.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06664427B1 |
| Source dataset | uspto-grants-2003_12 |
| ORD ID | ord-fc21bdecdfb54a22b3196ecf9c212560 |
| Source note | uspto-grants-2003_12 |