HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenyl Salicylate → 2'-Ethyl-salicylanilide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenyl Salicylate | HCID 8361 | — |
| Reactant | 2-Ethylaniline | HCID 11357 | — |
| Product | 2'-Ethyl-salicylanilide | HCID 18760914 | — |
Reaction Steps
The 2′-ethyl-salicylanilide was prepared by condensing phenyl salicylate with 2-ethylaniline then purified as described in Example 2a. The ligand mixture was then prepared from 2′-ethyl-salicylanilide and 1,1′-bi-2-naphthol using the procedure described in Example 2a. 31P NMR (121.77 MHz): several peaks between 117.1-118.8 ppm.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06664427B1 |
| Source dataset | uspto-grants-2003_12 |
| ORD ID | ord-4bbf13c0bf514f11b9c4464537d267e6 |
| Source note | uspto-grants-2003_12 |