HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenyl Salicylate → 2-Hydroxy-N-[2-(1-methylethyl)phenyl]benzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenyl Salicylate | HCID 8361 | — |
| Reactant | 2-Isopropylaniline | HCID 12561 | — |
| Product | 2-Hydroxy-N-[2-(1-methylethyl)phenyl]benzamide | HCID 7303341 | — |
Reaction Steps
The 2′-isopropyl-salicylanilide was prepared by condensing phenyl salicylate with 2-isopropylaniline then purified as described in Example 2a. The ligand mixture was then prepared from 2′-isopropyl-salicylanilide and binaphthol using the procedure described in Example 2a. 31P NMR (121.77 MHz): several peaks between 117.1-120.9 ppm.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06664427B1 |
| Source dataset | uspto-grants-2003_12 |
| ORD ID | ord-d1d59b24fdcc44119b80699fe89df6a1 |
| Source note | uspto-grants-2003_12 |