HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium methanethiolate → HCID 22320453, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium methanethiolate | HCID 4378561 | — |
| Reactant | HCID 22320437 | HCID 22320437 | — |
| Product | HCID 22320453 | HCID 22320453 | 93.5% |
Reaction Steps
Using the general method of Example 21 Part D, 2-butyl-1-(2-chloroethyl)-1H-imidazo[4,5-c]quinoline-4-amine (1.44 g, 4.76 mmol) was reacted with sodium thiomethoxide (0.42 g of 95%, 5.71 mmol) to provide 1.4 g of 2-butyl-1-[2-(methylthio)ethyl]-1H-imidazo[4,5-c]quinolin-4-amine as an off-white powder.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06667312B2 |
| Source dataset | uspto-grants-2003_12 |
| ORD ID | ord-162dd4ec43e8436996b277a53988c2e2 |
| Source note | uspto-grants-2003_12 |