HRID433396

反应详情

EQUATION

反应方程式

HRID 433396 的结构方程式

PROCEDURE

实验过程

Following General Procedure A above using N-(3,5-difluorophenylacetyl)-L-alanine (Example B) and 3-amino-1,3,4,5-tetrahydro-2H-1-benzazepin-2-one (General Procedure 6-B), the title compound was prepared. The reaction was monitored by tlc on silica gel (Rf=0.15 in 12% methanol/dichloromethane) and purification was by flash chromatography using 12% methanol/dichloromethane as the eluant.

WORKUP

后处理

  1. customThe reaction was monitored by tlc on silica gel (Rf=0.15 in 12% methanol/dichloromethane) and purification