HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 11552171, compound → HCID 10281772, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 11552171 | HCID 11552171 | — |
| Reactant | (2S)-2-[[2-(3,5-difluorophenyl)acetyl]amino]propanoic acid | HCID 12135350 | — |
| Solvent | Chloroform methanol | HCID 21584188 | — |
| Product | HCID 10281772 | HCID 10281772 | — |
Reaction Steps
Following General Procedure D and using N-(3,5-difluorophenylacetyl)-L-alanine (Ex. B) and 5-amino-7-phenbutyl-5,7-dihydro-6H-dibenz[b,d]azepin-6-one (Example 7-K), the title compound was prepared. The reaction was monitored by tlc (Rf=0.35, 3% MeOH/CHCl3) and product was purified by chromatography (silica, 3% MeOH/CHCl3).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06667305B1 |
| Source dataset | uspto-grants-2003_12 |
| ORD ID | ord-712045982f454cdabc68265a8d10fdf9 |
| Source note | uspto-grants-2003_12 |