3,5-Difluorophenylacetic acid → HCID 86584971, compound

Participants

Reaction Steps

Following General Procedure D above using 3,5-difluorophenylacetic acid (Oakwood Products, Inc.) and 3-(L-alaninyl)-amino-7-chloro-2,3-dihydro-1-methyl-5-phenyl-1H-1,4-benzodiazepin-2-one (Example 8-C), the title compound was prepared as a white solid having a melting point of 126.5-130° C. C27H23ClF2N4O3 (MW=524.1); mass spectroscopy 523.7. Anal. calcd for C27H23ClF2N4O3: C, 61.78; H, 4.42; N, 10.67. Found: C, 61.92; H, 4.52; N, 10.46.

Provenance & Evidence