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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 433426Generated: October 30, 2026

3,5-Difluorophenylacetic acid → HCID 22984114, compound

https://huagongshe.com/reaction/433426

Reaction equation

Participants

RoleNameHCIDCharge
Reactant3,5-Difluorophenylacetic acidHCID 145424—
ReactantHCID 23552778HCID 23552778—
ProductHCID 22984114HCID 22984114—

Reaction Steps

Following General Procedure D above using 3,5-difluorophenylacetic acid (Oakwood Products, Inc.) and 3-(L-tert-leucinyl)amino-2,3-dihydro-1-methyl-5-phenyl-1H-1,4-benzodiazepin-2-one (Example 8-Z), the title compound was prepared as a solid (mp.=221-222° C.). The product was purified by slurrying in ether.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06667305B1
Source datasetuspto-grants-2003_12
ORD IDord-f7d5c6eb99cb4011a0f67d31e1b97afb
Source noteuspto-grants-2003_12