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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 433428Generated: October 30, 2026

3,5-Difluorophenylacetic acid → HCID 22984066, compound

https://huagongshe.com/reaction/433428

Reaction equation

Participants

RoleNameHCIDCharge
Reactant3,5-Difluorophenylacetic acidHCID 145424—
ReactantHCID 23552780HCID 23552780—
ProductHCID 22984066HCID 22984066—

Reaction Steps

Following General Procedure D above using 3,5-difluorophenylacetic acid (Oakwood Products, Inc.) and 3-(L-alaninyl)amino-2,3-dihydro-1-cyclopropylmethyl-5-phenyl-1H-1,4-benzodiazepin-2-one (Example 8-L), the title compound was prepared as a solid (mp.=203-205° C.). The product was purified by slurrying in ether/hexanes.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06667305B1
Source datasetuspto-grants-2003_12
ORD IDord-3e42615dacc54091af78d032d56d50d7
Source noteuspto-grants-2003_12