huagongshe.com
HRID433489

反应详情

EQUATION

反应方程式

HRID 433489 的结构方程式

REACTANTS

反应物

2
结构：CC(=O)C(=O)OCC(C)C
HCID83084

Isobutyl pyruvate

C7H12O3

结构：Cc1ccc2cc(N)ccc2n1
HCID103148

6-Quinolinamine, 2-methyl-

C10H10N2

PRODUCTS

生成物

1
结构：Cc1ccc2cc(N[C@@H](C)C(=O)OCC(C)C)ccc2n1
HCID54119157

未命名化合物

PROCEDURE

实验过程

Following General Procedure AA above and using 6-amino-2-methylquinoline (Lancaster) and iso-butyl pyruvate (prepared by following General Procedure AO above), the title compound was prepared. The reaction was monitored by silica gel tlc (Rf=0.44 in 50% EtOAc/hexanes). Purification was by flash chromatography (silica gel using 50% EtOAc/hexanes as the eluant).

WORKUP

后处理

  1. customPurification