HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Methylimidazole → HCID 9815053, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Methylimidazole | HCID 12749 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | 4-chloromethyl-1-(3,4-dichloro-phenyl)-1H-pyrazole | HCID 23445015 | — |
| Product | HCID 9815053 | HCID 9815053 | — |
Reaction Steps
2-Methylimidazole was deprotonated with sodium hydride and then treated with 4-chloromethyl-1-(3,4-dichloro-phenyl)-1H-pyrazole. Extractive and chromatographic workup gave the title compound as a white crystalline solid. Mp. 176-177° C. (AcOEt), MS: m/e=307 (M+H+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06667335B2 |
| Source dataset | uspto-grants-2003_12 |
| ORD ID | ord-a0ed47f7dfc7452ab2457fea6e96e6ce |
| Source note | uspto-grants-2003_12 |