HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → 4-Chloromethyl-2-(3,4-dichloro-phenyl)-pyridine hydrochloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | [2-(3,4-Dichlorophenyl)pyridin-4-yl]methanol | HCID 23445072 | — |
| Product | 4-Chloromethyl-2-(3,4-dichloro-phenyl)-pyridine hydrochloride | HCID 23445010 | — |
Reaction Steps
The title compound, MS: m/e=271.0 (M+) was obtained as a light brown foam (100% yield) by the reaction of [2-(3,4-dichloro-phenyl)-pyridine-4-yl]-methanol with thionyl chloride at 20° C. for 1 h.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06667335B2 |
| Source dataset | uspto-grants-2003_12 |
| ORD ID | ord-17093c7e19e14216a21756db68f19ab6 |
| Source note | uspto-grants-2003_12 |