HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 23444948, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 23445057 | HCID 23445057 | — |
| Product | HCID 23444948 | HCID 23444948 | — |
Reaction Steps
The title compound, MS: m/e=245.1 (M+) was obtained as a yellow solid (98% yield) by the reaction of [5-(3,4-dimethyl-phenyl)-2-methyl-pyridin-3-yl]-methanol hydrochloride (1:1) with thionyl chloride at 20° C. for 1 h then 2 h at reflux.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06667335B2 |
| Source dataset | uspto-grants-2003_12 |
| ORD ID | ord-8b017f426e8244939119730019656c85 |
| Source note | uspto-grants-2003_12 |