HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
lithium aluminium hydride THF → [4-(3,4-Dichlorophenyl)-2-pyridinyl]methanol
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | lithium aluminium hydride THF | HCID 68718528 | — |
| Edukt | 4-(3,4-Dichloro-phenyl)-pyridine-2-carboxylic acid methyl ester | HCID 69038928 | — |
| Lösungsmittel | Tetrahydrofuran | HCID 8028 | — |
| Produkt | [4-(3,4-Dichlorophenyl)-2-pyridinyl]methanol | HCID 23445021 | — |
Reaktionsschritte
The title compound, MS: m/e=252.0 ([M-H]−) was obtained as a light brown oil (94% yield) by the reaction of 4-(3,4-dichloro-phenyl)-pyridine-2-carboxylic acid methyl ester with 1M lithium aluminum hydride/THF solution in THF at 20° C. for 1 h followed by chromatographic purification.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06667335B2 |
| Quelldatensatz | uspto-grants-2003_12 |
| ORD ID | ord-8d28d93c649840fb8a26cb755215164a |
| Quellennotiz | uspto-grants-2003_12 |