3,4-Dichlorobenzeneboronic acid → HCID 69043512, compound

HRID 433604Notes

Reaction equation

HRID 433604 reaction equation
[CH3:1][O:2][C:3]([C:5]1[CH:10]=[CH:9][CH:8]=[C:7](Br)[N:6]=1)=[O:4].[Cl:12][C:13]1[CH:14]=[C:15](B(O)O)[CH:16]=[CH:17][C:18]=1[Cl:19]>>[CH3:1][O:2][C:3]([C:5]1[CH:10]=[CH:9][CH:8]=[C:7]([C:16]2[CH:15]=[CH:14][C:13]([Cl:12])=[C:18]([Cl:19])[CH:17]=2)[N:6]=1)=[O:4]

Participants

3

Reactant 2

HCID 27343303,4-Dichlorobenzeneboronic acidHCID 16217886Methyl 6-bromopyridine-2-carboxylate

Product 1

HCID 69043512HCID 69043512, compound

Procedure

The title compound, MS: m/e=282.0 (M+) was obtained as a light yellow solid (7% yield) by the reaction of 6-bromo-pyridine-2-carboxylic acid methyl ester with 3,4-dichlorophenyl boronic acid.

Sources & evidence

ORD record
ord-20309de3b5ca4342bda152c16e0cb40c
Source dataset
uspto-grants-2003_12
Patent number
US06667335B2

Reaction notes

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