HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 9898883, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | HCID 12114314 | HCID 12114314 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 9898883 | HCID 9898883 | 101.6% |
Reaction Steps
A mixture of (S)-2-(2,3,5,6-tetrachloro-pyridin-4-ylamino)-propan-1-ol (6 g), 10% palladium on carbon (3 g), potassium carbonate (14.3 g) and ethanol (110 ml) was stirred under an atmosphere of hydrogen for 24 h. The reaction mixture was filtered through Harbolite™ and the filtrate was concentrated under reduced pressure to give the title compound as a white solid (3.2 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06670381B2 |
| Source dataset | uspto-grants-2003_12 |
| ORD ID | ord-14c0198b37ca43bd91ae740cc942c442 |
| Source note | uspto-grants-2003_12 |