HuagongsheHuagongshe Chemistry Print Report · For research reference only
Propargyl bromide → HCID 22254484, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Propargyl bromide | HCID 7842 | — |
| Reactant | 2-Octyl-1H-imidazo[4,5-c]quinoline-1-ethanol | HCID 22254501 | — |
| Product | HCID 22254484 | HCID 22254484 | 90.3% |
Reaction Steps
Using the general method of Example 1 Part A, 2-(2-octyl-1H-imidazo[4,5-c]quinolin-1-yl)ethanol (4.8 g, 14.75 mmol) was reacted with propargyl bromide (80% in toluene, 4.93 mL, 44.25 mmol) to provide 4.84 g of 2-octyl-1-[2-(prop-2-ynyloxy)ethyl]-1H-imidazo[4,5-c]quinoline as a brown solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06670372B2 |
| Source dataset | uspto-grants-2003_12 |
| ORD ID | ord-183ab53c65944b8cad409ec1490e2697 |
| Source note | uspto-grants-2003_12 |