HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetyl chloride → Sarcosine piperonyl amide hydrochloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetyl chloride | HCID 6367 | — |
| Reactant | N-Boc sarcosine piperonylamide | HCID 86586337 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | Sarcosine piperonyl amide hydrochloride | HCID 69348013 | — |
Reaction Steps
N-Boc sarcosine piperonylamide (500 mg, 1.54 mmol) in methanol (10 mL) was treated with acetyl chloride (1 mL). After 45 minutes, all volatiles were removed under reduced pressure to yield sarcosine piperonyl amide hydrochloride (395 mg, quant.) as a sticky solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06670473B2 |
| Source dataset | uspto-grants-2003_12 |
| ORD ID | ord-25aef67b5e524bbfa3a8051233b351bc |
| Source note | uspto-grants-2003_12 |