反应详情

To a solution of 1.26 g (0.01 mol) of anhydrous manganese chloride was added 4.5 g (0.03 mol) of 1,2-benzisothiazolin in 30 ml of water. The solution was concentrated to give a tan colored solid. The solid was thoroughly washed with dry acetone, filtered and dried at room temperature to yield 3.47 g (77%) of product, m.p. >250° C.

1. concentrationThe solution was concentrated
2. customto give a tan colored solid
3. washThe solid was thoroughly washed with dry acetone
4. filtrationfiltered
5. customdried at room temperature