HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethylamine → 2-Cyanoethyl trans-3-diethylaminoacrylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethylamine | HCID 8021 | — |
| Reactant | 2-Cyanoethyl prop-2-ynoate | HCID 20493224 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | 2-Cyanoethyl trans-3-diethylaminoacrylate | HCID 20493226 | — |
Reaction Steps
A solution of 48 g (0.39 moles) of 2-cyanoethyl propiolate in 100 ml of chloroform was treated with a solution of 28.5 g (0.38 moles) of diethylamine in 100 ml of chloroform. The temperature was kept at 10° to 20° C. during the addition. The chloroform was stripped off and the product used without purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04396546 |
| Source dataset | uspto-grants-1983_08 |
| ORD ID | ord-bba4eff755de40e483cb36529d0fda20 |
| Source note | uspto-grants-1983_08 |