Isopropanol → HCID 10945389, compound

Participants

Reaction Conditions

Reaction Steps

A mixture of 3.09 g of dicyclohexylcarbodiimide, 30 mg of cuprous chloride and 994 mg of isopropanol was stirred under an inert atmosphere at 55° C. for 6 hours and was then diluted with ethyl acetate. The organic phase was washed with water, then with N ammonium hydroxide solution, was dried and filtered. The filtrate was evaporated to dryness under reduced pressure to obtain 3.2 g of O-isopropyl-N,N'-dicyclohexyl-isourea which was used as is for the next step.

Provenance & Evidence