Zincchloride → HCID 178478907, compound

HRID 434348Notes

Reaction equation

HRID 434348 reaction equation
[CH:1]1([C:7]2[CH:12]=[CH:11][C:10]([N:13]=[C:14]3[NH:19][CH2:18][CH2:17][CH2:16][NH:15]3)=[CH:9][CH:8]=2)[CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1.[Cl-:20].[Zn+2:21].[Cl-]>C(#N)C>[Cl-:20].[Zn+2:21].[CH:1]1([C:7]2[CH:12]=[CH:11][C:10]([N:13]=[C:14]3[NH:15][CH2:16][CH2:17][CH2:18][NH:19]3)=[CH:9][CH:8]=2)[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6]1.[Cl-:20]

Participants

4

Reactant 2

HCID 3007855ZincchlorideHCID 178419944HCID 178419944, compound

Product 1

HCID 178478907HCID 178478907, compound

Reagents, catalysts & solvents 1

HCID 6342AcetonitrileSolvent2×

Procedure

10.3 g of 2-(4-cyclohexylphenyl)imino-hexahydropyrimidine are dissolved in 150 ml of warm acetonitrile. To this solution is added a warm solution of 2.7 g of zinc-chloride in acetonitrile. The solvent is then evaporated after which the 2-(4-cyclohexylphenyl)imino-hexahydropyrimidine zinc chloride complex is obtained. The complex is characterized by the I.R.-spectrum.

Workup

  1. customThe solvent is then evaporated after which the 2-(4-cyclohexylphenyl)imino-hexahydropyrimidine zinc chloride complex
  2. customis obtained

Sources & evidence

ORD record
ord-b42fea7601154edc9313ca94105ec94a
Source dataset
uspto-grants-1983_08
Patent number
US04396617

Reaction notes

Loading…