反应详情

Sodium borohydride (10.0 g) was added portionwise to an ice cold stirred solution of 1-phenylpropan-2-one (30.0 g) in methanol (500 ml). The mixture was stirred for 4 hours, evaporated and partitioned between water (100 ml) and chloroform (200 ml). The organic phase was dried (MgSO4) and evaporated to give the product as a colourless oil (26.4 g).

1. customevaporated
2. custompartitioned between water (100 ml) and chloroform (200 ml)
3. dry with materialThe organic phase was dried (MgSO4)
4. customevaporated