HuagongsheHuagongshe Chemistry Print Report · For research reference only
Catechol → HCID 14171516, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Catechol | HCID 289 | — |
| Reactant | 2-(Chloromethyl)-2-phenyloxirane | HCID 200204 | — |
| Product | HCID 14171516 | HCID 14171516 | — |
Reaction Steps
Catechol and 2-phenyl epichlorohydrin were reacted to give the intermediate 2-hydroxymethyl-2-phenyl-1,4-benzodioxan (method (a) of Example 2) which was converted to the imidazoline compound by method (b) of Example 2. The free base was recrystallised from light petroleum (60°-80°); m.p. 114.5°-116°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04397860 |
| Source dataset | uspto-grants-1983_08 |
| ORD ID | ord-d3a7886f753b4916b850ec968f55e5a5 |
| Source note | uspto-grants-1983_08 |