HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → HCID 178503555, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | 4-Imidazolidinone,5-methyl-2-thioxo-(9CI) | HCID 3032907 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 178503555 | HCID 178503555 | 57% |
Reaction Steps
A solution of 5-methyl-2-thiohydantoin (15 g.) and methyl iodide (16.3 g.) in dry ethanol (130 ml.) was heated under reflux for 11/2 hours, and then allowed to stand at 0° overnight. The crystalline product was filtered and washed with ether to give 2-methylthio-5-methyl-2-imidazolin-4-one hydroiodide (17.8 g.), m.p. 170°-173°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04399142 |
| Source dataset | uspto-grants-1983_08 |
| ORD ID | ord-3827c7e781164fe1b9aaaf0c56c3d104 |
| Source note | uspto-grants-1983_08 |