HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-bromobutanimide → HCID 86738980, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-bromobutanimide | HCID 67184 | — |
| Reactant | HCID 13371596 | HCID 13371596 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 86738980 | HCID 86738980 | 70.4% |
Reaction Steps
By proceeding as described in Example 1 but using 800 mg of N-bromosuccinimide and 1.47 g of (5Z,13E)-(9α,11α,15R)-9,11,15-trihydroxy-16,16-dimethylprosta-5,13-dienoic acid methyl ester dissolved in a mixture of 40 ml of chloroform and 4 ml of tetrahydrofuran, there was obtained 1.24 g of the title compound having the following physical characteristics:
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04399147 |
| Source dataset | uspto-grants-1983_08 |
| ORD ID | ord-aab2dd0949d447b1941d57a7f709e569 |
| Source note | uspto-grants-1983_08 |