Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 434733Generated: October 29, 2026

N-bromobutanimide → HCID 86738980, compound

https://huagongshe.com/reaction/434733

Reaction equation

Participants

RoleNameHCIDCharge
ReactantN-bromobutanimideHCID 67184—
ReactantHCID 13371596HCID 13371596—
SolventChloroformHCID 6212—
SolventTetrahydrofuranHCID 8028—
ProductHCID 86738980HCID 8673898070.4%

Reaction Steps

By proceeding as described in Example 1 but using 800 mg of N-bromosuccinimide and 1.47 g of (5Z,13E)-(9α,11α,15R)-9,11,15-trihydroxy-16,16-dimethylprosta-5,13-dienoic acid methyl ester dissolved in a mixture of 40 ml of chloroform and 4 ml of tetrahydrofuran, there was obtained 1.24 g of the title compound having the following physical characteristics:

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04399147
Source datasetuspto-grants-1983_08
ORD IDord-aab2dd0949d447b1941d57a7f709e569
Source noteuspto-grants-1983_08