反应详情

50 g of 2,2-dimethylsuccinic acid and 70 ml of acetic anhydride were reacted at 140° C. for 3 hours and, after removing acetic acid and acetic anhydride under reduced pressure, the residue was subjected to vacuum distillation to obtain 37 g of 2,2-dimethylsuccinic anhydride.

1. customafter removing acetic acid and acetic anhydride under reduced pressure
2. distillationthe residue was subjected to vacuum distillation