Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Sodium Carbonate → N-Hydroxy-5-norbornene-2,3-dicarboxylic acid imide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Sodium Carbonate | HCID 10340 | — |
| 반응물 | 826-62-0 | HCID 13223 | — |
| 반응물 | Hydroxyamine hydrochloride | HCID 443297 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | N-Hydroxy-5-norbornene-2,3-dicarboxylic acid imide | HCID 178524005 | — |
반응 단계
30 ml of water was added to 24.6 g of 5-norbornene-2,3-dicarboxylic acid anhydride, and while cooling the reaction temperature below 20° C., 10.6 g of sodium carbonate and then 13.9 g of hydroxylamine hydrochloride were added. The mixture was reacted at room temperature for 1 hour and then reacted at a temperature of 60° to 70° C. for 1 hour. After cooling to room temperature, N-hydroxy-5-norbornene-2,3-dicarboxylic acid imide thus formed was collected by filtration.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04399210 |
| 출처 데이터셋 | uspto-grants-1983_08 |
| ORD ID | ord-6b46f60f07d04d8f8b24b76804aa1cb2 |
| 출처 메모 | uspto-grants-1983_08 |