HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyclohexyl bromide → Ethyl 2-[(cyclohexyloxy)imino]-3-oxobutanoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyclohexyl bromide | HCID 7960 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | HCID 178472877 | HCID 178472877 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | Ethyl 2-[(cyclohexyloxy)imino]-3-oxobutanoate | HCID 54351806 | 91.9% |
Reaction Steps
Ethyl 2-hydroxyimino-3-oxobutyrate (syn isomer, 30 g.), N,N-dimethylformamide (100 ml.), potassium carbonate (39.5 g.) and cyclohexyl bromide (31.1 g.) were treated in a similar manner to that of Example F-(1) to give ethyl 2-cyclohexyloxyimino-3-oxobutyrate (syn isomer, 41.8 g.), oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04399133 |
| Source dataset | uspto-grants-1983_08 |
| ORD ID | ord-b5b1590ad1d044d99cb44dbbab6ca8dd |
| Source note | uspto-grants-1983_08 |