HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 20490686, compound → HCID 20490674, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 20490686 | HCID 20490686 | — |
| Reactant | HCID 178418287 | HCID 178418287 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 20490674 | HCID 20490674 | 100% |
Reaction Steps
The alcohol of Example 3(16 g), methylene chloride (300 ml) and pyridinium chlorochromate (14.5 g) were stirred over two days at room temperature. The solution was filtered through a column of Fluorosil using methylene chloride as eluant. Evaporation of the solvent gave 15.8 g, corresponding a 100% yield, of the desired product, which solidified on cooling.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04400198 |
| Source dataset | uspto-grants-1983_08 |
| ORD ID | ord-74f9355fc3a84ec8b2804113ea719e00 |
| Source note | uspto-grants-1983_08 |