Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Formaldehyde | HCID 712 | — |
| Reactant | Oxalic Acid | HCID 971 | — |
| Reactant | Phenol | HCID 996 | — |
| Reactant | 4-Tert-octylphenol | HCID 8814 | — |
| Solvent | O-Xylene | HCID 7237 | — |
| Solvent | HCID 68147410 | HCID 68147410 | — |
| Product | HCID 86738988 | HCID 86738988 | — |
Reaction Steps
375 g. (1.8 moles) of p-tert-octylphenol, 75 g (0.8 mole) of phenol, 50 g (0.22 mole) of 4,4'-isopropylidene-biphenol (bisphenol A), 215 g (2.65 moles) of 37% formalin, 10 g of oxalic acid and 100 g of xylene were put into a reactor, and they were refluxed for 7 hours at the boiling point of the water-xylene azeotrope. The reaction mixture was then heated to 170° C. while removing water and the solvent, thereby giving a p-tert-octylphenol/phenol/bisphenol A/formaldehyde co-condensate having a softening point of 85° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US04400492 |
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| Source dataset | uspto-grants-1983_08 |
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| ORD ID | ord-896fc68a14ec47a180ba5d7bb7682ab0 |
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| Source note | uspto-grants-1983_08 |
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