HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sulfuryl chloride → Ethyl 2-iso-butoxyimino-4-chloro-3-oxobutyrate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sulfuryl chloride | HCID 24648 | — |
| Reactant | Ethyl 2-[(2-methylpropoxy)imino]-3-oxobutanoate | HCID 53699031 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | Ethyl 2-iso-butoxyimino-4-chloro-3-oxobutyrate | HCID 54168146 | 65.5% |
Reaction Steps
Ethyl 2-iso-butoxyimino-3-oxobutyrate (syn isomer, 42 g.), acetic acid (42 ml.) and sulfuryl chloride (27.1 g.) were treated in a similar manner to that of Example F-(2) to give ethyl 2-iso-butoxyimino-4-chloro-3-oxobutyrate (syn isomer, 31.9 g.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04400379 |
| Source dataset | uspto-grants-1983_08 |
| ORD ID | ord-b0ec8f563e4948f3a13308879bbc41a6 |
| Source note | uspto-grants-1983_08 |