HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Azide → HCID 54355517, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Azide | HCID 33557 | — |
| Reactant | 6-(3-Chloropropyl)-6-(2-methoxyethoxy)-2,5,7,10-tetraoxa-6-silaundecane | HCID 15006778 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 54355517 | HCID 54355517 | — |
Reaction Steps
1.0 mole of 3-chloropropyltris(methoxyethoxy)-silane and 1.1 moles of sodium azide in 500 ml of acetonitrile were heated in the presence of 5 mole percent of the catalyst described in Example 1 (a) for eight hours under reflux and stirring. After separation of the salt the subsequent distillation under reduced pressure gave the 3-azidopropyltris(methoxyethoxy)silane in a yield of 84 weight percent with the following characteristics:
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04401598 |
| Source dataset | uspto-grants-1983_08 |
| ORD ID | ord-943482ba272846b296b1d19e86991a05 |
| Source note | uspto-grants-1983_08 |