HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Chlorophenol → HCID 13041344, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Chlorophenol | HCID 7933 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | 18-Crown-6 | HCID 28557 | — |
| Reactant | N-(1-methylethyl)-3-phenyl-2-oxiranecarboxamide | HCID 13041334 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 13041344 | HCID 13041344 | — |
Reaction Steps
This compound was prepared from N-(1-methylethyl)-3-phenyl-2-oxiranecarboxamide (6.16 g.) m-chlorophenol (3.9 g.), sodium hydride (50% oil dispersion, 1.5 g.), 18-crown-6 (0.9 g.), and acetonitrile (250 ml.) as described in Example 12. The product which was purified by recrystallization from ether melted at 151°-153°, and weighed 1.4 g.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04401832 |
| Source dataset | uspto-grants-1983_08 |
| ORD ID | ord-05e81c9f9fb84dc493342cb13729695a |
| Source note | uspto-grants-1983_08 |