Methyl iodide → HCID 70639049, compound

HRID 435569Notes

Reaction equation

HRID 435569 reaction equation
[CH3:1][N:2]1[CH:6]=[CH:5][N:4]=[C:3]1[CH3:7].[CH3:8][I:9]>CCOCC>[I-:9].[CH3:1][NH+:2]1[CH:6]=[CH:5][N:4]([CH3:8])[CH:3]1[CH3:7]

Participants

4

Reactant 2

HCID 6328Methyl iodideHCID 156171,2-Dimethylimidazole

Product 1

HCID 70639049HCID 70639049, compound

Reagents, catalysts & solvents 1

HCID 3283Diethyl EtherSolvent

Procedure

To 20 g of 1,2-dimethylimidazole dissolved in 100 ml of ether there is added 20 ml of methyl iodide. On standing the product precipitates and is filtered off. Two crystallizations from ethanol-ether furnish the pure product, melting point 315°-318° C.

Workup

  1. customprecipitates
  2. filtrationis filtered off
  3. customTwo crystallizations from ethanol-ether
  4. customfurnish the pure product, melting point 315°-318° C.

Sources & evidence

ORD record
ord-399755a8c65547b493250a524692e62f
Source dataset
uspto-grants-1977_02
Patent number
US04006137

Reaction notes

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