HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 70638847, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | 4-Chlorobenzaldehyde | HCID 7726 | — |
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | HCID 70639049 | HCID 70639049 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 70638847 | HCID 70638847 | 59.6% |
Reaction Steps
A mixture of 6.0 g of 1,2,3-trimethyl-1H-imidazolium iodide, 1g of potassium hydroxide, and 6 g of p-chlorobenzaldehyde is refluxed in 25 ml of absolute ethanol for 15 minutes during which time a precipitate is formed. The reaction mixture is cooled, 5 ml of water is added, and the solid is filtered off and dried. Crystallization from absolute ethanol yields 5.4 g of the title compound, melting point 266°-268° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04006137 |
| Source dataset | uspto-grants-1977_02 |
| ORD ID | ord-748d1f7fdea1441082335393191ff8f3 |
| Source note | uspto-grants-1977_02 |