HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → HCID 70638075, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | HCID 70638589 | HCID 70638589 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 70638075 | HCID 70638075 | — |
Reaction Steps
1,3-Dimethyl-2-[2-(2-pyridinyl)ethenyl]-1H-imidazolium iodide (6.5 g) and 10 ml of methyl iodide are refluxed in 20 ml of acetonitrile for one hour. The resulting solid is filtered off and crystallized from methanol to yield 5.5 g of the title compound, melting point 75° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04006137 |
| Source dataset | uspto-grants-1977_02 |
| ORD ID | ord-d3f77fe4528949b0b83b666af4029d07 |
| Source note | uspto-grants-1977_02 |