HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Bromide → HCID 178526341, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Bromide | HCID 253877 | — |
| Reactant | Diisobutylaluminumhydride | HCID 21225700 | — |
| Reactant | HCID 21767799 | HCID 21767799 | — |
| Reactant | HCID 178471293 | HCID 178471293 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 178526341 | HCID 178526341 | — |
Reaction Steps
Treatment of 2-(4-carbethoxybutyl)-2-cyclopentenone as methoxime (Example 24) with diisobutyl aluminum hydride in the manner described in Example 17 gives crystals, m.p. 33°-35° C. IR (KBr) 3420, 1630, 1050, 886 cm-1. λ MeOH/max 243 (12,020).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04006179 |
| Source dataset | uspto-grants-1977_02 |
| ORD ID | ord-45458782734a45d6943b55601ad8c2cc |
| Source note | uspto-grants-1977_02 |