Pyridinium chloride → HCID 21455080, compound

HRID 436008Notes

Reaction equation

[CH2:1]([C:3]1[S:7][C:6]2[CH:8]=[CH:9][CH:10]=[CH:11][C:5]=2[C:4]=1[C:12](=[O:23])[C:13]1[CH:18]=[C:17]([CH3:19])[C:16]([O:20]C)=[C:15]([CH3:22])[CH:14]=1)[CH3:2].Cl.N1C=CC=CC=1>>[CH2:1]([C:3]1[S:7][C:6]2[CH:8]=[CH:9][CH:10]=[CH:11][C:5]=2[C:4]=1[C:12](=[O:23])[C:13]1[CH:18]=[C:17]([CH3:19])[C:16]([OH:20])=[C:15]([CH3:22])[CH:14]=1)[CH3:2]

Participants

Reactant 2

HCID 10176127Pyridinium chloride

HCID 21455079HCID 21455079, compound

Product 1

HCID 21455080HCID 21455080, compound

Procedure

Into a half-litre flask equipped with a condenser, a mechanical stirrer and a thermometer, 25 g (0.777 mol) of 2-ethyl-3-(3,5-dimethyl-4-methoxy-benzoyl)benzo[b]thiophene were introduced with 125 g of pyridine hydrochloride.

Workup

customInto a half-litre flask equipped with a condenser, a mechanical stirrer

Sources & evidence

ORD record: ord-b14af02c48294304b41ff6fa6ee63471
Source dataset: uspto-grants-1977_02
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04007204

Reaction notes

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