Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Toluene | HCID 1140 | — |
| Reactant | 1-Iodo-3-(p-anisyldiphenylmethoxy)-trans-1-octene | HCID 20144623 | — |
| Reactant | Butyllithium | HCID 178418339 | — |
| Solvent | Hexane | HCID 8058 | — |
| Product | HCID 178506900 | HCID 178506900 | — |
Reaction Steps
To a solution of 5.26 g. of 1-iodo-3-(p-anisyldiphenylmethoxy)-trans-1-octene (Example 956) in 10 ml. of toluene, cooled to -78° C., is added under an inert atmosphere 1 molar equivalent of n-butyllithium dissolved in hexane. The reaction mixture is allowed to warm to -40° C. and is maintained at that temperature for 1 hour to yield a hydrocarbon solution of 3-(p-anisyldiphenylmethoxy)-trans-1-octenyllithium.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04007210 |
|---|
| Source dataset | uspto-grants-1977_02 |
|---|
| ORD ID | ord-f58854390ecf4df8b50fc2415bc2dc27 |
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| Source note | uspto-grants-1977_02 |
|---|
