HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diisopropyl Ether → 2-Ethylamino-5H-s-triazolo[5,1-a]isoindole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diisopropyl Ether | HCID 7914 | — |
| Reactant | Aluminium lithium hydride | HCID 21226445 | — |
| Reactant | 2-Acetamido-5H-s-triazolo[5,1-a]isoindole | HCID 21455274 | — |
| Solvent | 1,2-Dimethoxyethane | HCID 8071 | — |
| Product | 2-Ethylamino-5H-s-triazolo[5,1-a]isoindole | HCID 21455282 | 60% |
Reaction Steps
2-Acetamido-5H-s-triazolo[5,1-a]isoindole is reduced with lithium aluminum hydride at 0-10°C in dimethoxyethane. Yield 60%. M.p. 150-2°C (isopropyl ether).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04007276 |
| Source dataset | uspto-grants-1977_02 |
| ORD ID | ord-1698e8343a5d4194b67064ab35228daa |
| Source note | uspto-grants-1977_02 |