HuagongsheHuagongshe Chemistry Print Report · For research reference only
Furfuryl Alcohol → Furfuryl acetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Furfuryl Alcohol | HCID 7361 | — |
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Solvent | Triethylamine | HCID 8471 | — |
| Product | Furfuryl acetate | HCID 12170 | 99.5% |
Reaction Steps
Procedure was as in example 2, but acetic anhydride was added to the mixture of furfuryl alcohol and triethyl amine. The crude yield was 1149 g and the concentration was 58.7%, i.e., the yield was 99.5%. The crude product was washed 4 times with 200 ml water, whereby 641.3 g furfuryl acetate was obtained, its concentration was 96.2%, i.e., the yield was 91.0%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04008256 |
| Source dataset | uspto-grants-1977_02 |
| ORD ID | ord-926e23620bc040f0978634dc078eb382 |
| Source note | uspto-grants-1977_02 |