Sodium Hydroxide → HCID 54432175, compound

HRID 436337Notes

Reaction equation

HRID 436337 reaction equation
[N+:1]([C:4]1[CH:16]=[CH:15][C:7]([NH:8][CH2:9][CH2:10][NH:11][C:12]([NH2:14])=[O:13])=[C:6]([O:17][CH3:18])[CH:5]=1)([O-])=O.[OH-].[Na+].S(S([O-])=O)([O-])=O.[Na+].[Na+]>>[NH2:1][C:4]1[CH:16]=[CH:15][C:7]([NH:8][CH2:9][CH2:10][NH:11][C:12]([NH2:14])=[O:13])=[C:6]([O:17][CH3:18])[CH:5]=1

Participants

4

Reactant 3

HCID 14798Sodium HydroxideHCID 24489Sodium DithioniteHCID 21454198HCID 21454198, compound

Product 1

HCID 54432175HCID 54432175, compound

Procedure

30 g (0.118 mole) of 4-nitro-2-methoxy-N-(β-ureidoethyl) aniline is introduced little by little, while stirring and cooling, sufficiently to avoid any increase in temperature into 300 cm3 of a 3N solution of sodium hydroxide to which 120 g of sodium hydrosulfite has been added and which has been brought to 70° C.

Workup

  1. temperaturecooling
  2. additionhas been added
  3. customhas been brought to 70° C.

Sources & evidence

ORD record
ord-36bc80e047674fa4b33f580a04b742fe
Source dataset
uspto-grants-1977_02
Patent number
US04008272

Reaction notes

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