Benzene → HCID 11830208, compound

HRID 436370Notes

Reaction equation

HRID 436370 reaction equation
[C:1]1(=[O:8])[O:7][C:5](=[O:6])[CH2:4][C:2]1=[CH2:3].[Cl-].[Al+3].[Cl-].[Cl-].[CH:13]1[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=1>>[CH2:3]=[C:2]([CH2:4][C:5](=[O:6])[C:13]1[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=1)[C:1]([OH:7])=[O:8]

Participants

4

Reactant 3

HCID 241BenzeneHCID 75110Itaconic AnhydrideHCID 6451240Aluminum(III) Chloride

Product 1

HCID 11830208HCID 11830208, compoundYield 70%

Procedure

From itaconic anhydride treated with a large excess of benzene in the presence of aluminum chloride, there is recovered with a yield of about 70% the derivative of the formula: ##STR8##

Workup

  1. customis recovered with a yield of about 70% the derivative of the formula

Sources & evidence

ORD record
ord-0411bc22afc64787b779e283266f0af4
Source dataset
uspto-grants-1977_02
Patent number
US04008323

Reaction notes

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