HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrazine → 4-Chlorobenzoin hydrazone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrazine | HCID 9321 | — |
| Reactant | 1-(4-Chlorophenyl)-2-phenyl-1,2-ethanedione | HCID 89801 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 4-Chlorobenzoin hydrazone | HCID 86734502 | 62.8% |
Reaction Steps
To a solution of 3.5 g 4-chlorobenzil in 15 ml ethanol is added 0.45 g anhydrous hydrazine. The solution is refluxed for 1 hour, filtered and water added to the cloud point, and allowed to crystallize yielding 2.3 g of 4-chlorobenzoin hydrazone.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04009022 |
| Source dataset | uspto-grants-1977_02 |
| ORD ID | ord-cf6784566b12447d879fe85032a22105 |
| Source note | uspto-grants-1977_02 |