Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Potassium Hydroxide → HCID 21452975, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Potassium Hydroxide | HCID 14797 | — |
| 반응물 | 1,8-Octanediamine | HCID 24250 | — |
| 반응물 | 4-(Trifluoromethoxy)benzoyl Chloride | HCID 142110 | — |
| 용매 | 1,2-Dichloroethane | HCID 11 | — |
| 생성물 | HCID 21452975 | HCID 21452975 | — |
반응 단계
m.p. 164°-165° C., 12.0 g., was prepared as in Example 16 using 4-trifluoromethoxybenzoyl chloride (from 16.5 g. of 4-trifuoromethoxybenzoic acid as in Example 16) in 150 ml. of ethylene dichloride, 7.2 g. of 1,8-octanediamine, 200 ml. of 10% aqueous potassium hydroxide solution, 500 ml. of ethylene dichloride and recrystallization from methanol using decolorizing charcoal.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04009208 |
| 출처 데이터셋 | uspto-grants-1977_02 |
| ORD ID | ord-4328c9115ca741f790597127e260cedf |
| 출처 메모 | uspto-grants-1977_02 |