HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cystamine Dihydrochloride → N,N'-(Dithiodiethylene)bis(4-trifluoromethoxybenzamide)
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cystamine Dihydrochloride | HCID 5941 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | 4-(Trifluoromethoxy)benzoyl Chloride | HCID 142110 | — |
| Solvent | 1,2-Dichloroethane | HCID 11 | — |
| Product | N,N'-(Dithiodiethylene)bis(4-trifluoromethoxybenzamide) | HCID 21453017 | — |
Reaction Steps
m.p. 150°-151° C., 14.5 g., was prepared as in Example 1 using 33.6 g. of 4-trifluoromethoxybenzoyl chloride in 100 ml. of ethylene dichloride, 11.3 g. of cystamine dihydrochloride, 300 ml. of 10% sodium hydroxide solution, 400 ml. of ethylene dichloride and recrystallization from acetonitrile using decolorizing charcoal.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04009208 |
| Source dataset | uspto-grants-1977_02 |
| ORD ID | ord-6f459ac2cfe64807a84e0880839d34fc |
| Source note | uspto-grants-1977_02 |