HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Hydroxide → N,N'-Nonamethylenebis(4-trifluoromethoxybenzamide)
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | Nonamethylenediamine | HCID 69534 | — |
| Reactant | 4-(Trifluoromethoxy)benzoyl Chloride | HCID 142110 | — |
| Solvent | 1,2-Dichloroethane | HCID 11 | — |
| Product | N,N'-Nonamethylenebis(4-trifluoromethoxybenzamide) | HCID 21452865 | — |
Reaction Steps
m.p. 144°-145° C., 12.1 g., was prepared as in Example 1 using 24.6 of 4-trifluoromethoxybenzoyl chloride in 200 ml. ethylene dichloride, 7.9 g. of 1,9-nonanediamine, 60 ml. of 10% aqueous potassium hydroxide solution, 300 ml. of ethylene dichloride and recrystallization from acetonitrile.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04009208 |
| Source dataset | uspto-grants-1977_02 |
| ORD ID | ord-b050f254087d48e1acba345f61c99547 |
| Source note | uspto-grants-1977_02 |